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The SFE may be carried out in either static or dynamic mode. The pressure in the system is maintained by means of a restrictor (either fixed or variable, the latter making the pressure independent of the flow rate). At the end of the restrictor, the fluid is depressurized and the extracted analytes are trapped in an organic solvent or on a solid phase filled cartridge (from which the analytes are later eluted with a small volume of organic solvent).. Due to the numerous parameters affecting the extraction efficiencies, SFE affords a high degree of selectivity and it is this reason that supercritical fluid extraction has a wide range of industrial-scale uses. However, on the other hand, this makes the optimisation quite tedious and difficult in practice and maybe prevent all potential species being extracted.. The parameters to consider are linked to the extraction parameters inside the cell, to the nature of the solutes or to the nature of the matrix. The important parameters in SFE are both the ...

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A preparatory supercritical extraction cartridge includes a chamber for sample having a volume in the range of 20 cubic centimeters to 2,000 cubic centimeters. An inlet and an outlet are fastened to the cartridge walls by threads and sealed to said cartridge walls With spring loaded seals so that they can be removed with a torque requirement of less than 35 pound inches. Inlet and outlet tubing are fastened to the inlet and outlet by quick release connectors.

5.1 Exposure data. Oxazepam is a benzodiazepine used extensively since the 1960s for the treatment of anxiety and insomnia and in the control of symptoms of alcohol withdrawal. It is a metabolite of diazepam, prazepam and temazepam, among the benzodiazepines considered in this volume.. 5.2 Human carcinogenicity data. In one case-control study evaluating benzodiazepine use, subjects using oxazepam were included, but were too few to analyse as a separate category.. 5.3 Animal carcinogenicity data. Oxazepam was tested for carcinogenicity in three experiments in two strains of mice by oral administration in the diet. Significant increases in the incidence of benign and malignant liver tumours were found in two of the studies. The incidence of an uncommon malignant liver tumour, hepatoblastoma, was also increased in one strain of mice. In the third study, an increased incidence of liver adenomas was found. In one of the studies, a small increase in the incidence of thyroid gland adenomas was observed ...

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This application note compares the use of SFE and its competing technique, PSE, using the same universal instrument for the removal of gamma-tocopherol from walnuts.

Gamma-Tocopherol is the dominant form of Vitamin E in many commonly ingested foods in the human diet, such as plant seeds and nuts. In the past, supplement companies have focused on the health benefits of alpha-tocopherol.

TY - JOUR. T1 - Application of supercritical fluid extraction to components of crude drugs and plants. III. Extraction of pigments from lithospermum root and licorice root. AU - Manabe, A.. AU - Tokumori, T.. AU - Sumida, Y.. AU - Yoshida, T.. AU - Hatano, T.. AU - Yazaki, K.. AU - Okuda, T.. PY - 1987/1/1. Y1 - 1987/1/1. UR - http://www.scopus.com/inward/record.url?scp=0023179119&partnerID=8YFLogxK. UR - http://www.scopus.com/inward/citedby.url?scp=0023179119&partnerID=8YFLogxK. U2 - 10.1248/yakushi1947.107.7_506. DO - 10.1248/yakushi1947.107.7_506. M3 - Article. C2 - 3694459. AN - SCOPUS:0023179119. VL - 107. SP - 506. EP - 510. JO - Yakugaku Zasshi. JF - Yakugaku Zasshi. SN - 0031-6903. IS - 7. ER - ...

Waters Supercritical Fluid Extraction (SFE) systems extract chemical compounds using supercritical fluid instead of an organic solvent. The result is an extract with little or no residual solvent, superior purity and yield, and lower operating costs.

The magnitude of the contaminated site clean-up in the United States indicates the need for more effective, less costly remediation technologies. Supercritical Fluid Extraction (SFE) using carbon dioxide (CO2) as a supercritical fluid is a possible alternative technology for remediation of soils contaminated with volatile organic compounds. The feasibility of this process is mainly dependent on two factors: the extent and extraction rate of heavy molecular weight organic compounds from soil by supercritical carbon dioxide (SC-CO2). This paper presents results of a bench-scale study for remediation of soils contaminated with naphthalene and 1,2,4 trimethyl benzene as a function of the flow rate (QCO2) and supercritical fluid density (pCO2). These data are used to perform a basic economic analysis of the process by using these two organics selected as model soil contaminants. An additional aim of this study was to develop scale-up methodology from laboratory SFE devices to industrially ...

The piquant and peppery flavor of American Blue and Roquefort cheese is largely due to the short and medium chain fatty acids, methyl ketones and secondary alcohols. The free fatty acids contribute flavor themselves and are also precursors of methyl ketones. Lipase action during the cheese ripening leads to formation of free fatty acids (FFA). The short chain FFA (C6 to C10) are more peppery in flavor than long chain FFA. Conventional methods of FFA analysis suffer from limitations such as loss of volatile fatty acids during derivatization of samples and difficulties in extraction and separation of short, medium and long chain fatty acids in a single analysis. Enhanced FFA recoveries from spiked matrix samples were obtained at 680 atm by SFE/SFC procedure with a 5% methanol modifier containing 1% acetic acid. A procedure was developed utilizing supercritical fluid extraction to isolate the FFA and subsequently separate and quantitate the FFA with supercritical fluid chromatography. The ...

Supercritical fluid extraction (SFE) was used to extract total alkaloids, peimisine, peimine and peiminine from the bulb of Fritillaria thunbergii Miq. The antioxidant capacity of the extracts was evaluated by DPPH radical scavenging activity (DPPH-RSA), ABTS radical scavenging activity (ABTS-RSA) and ferric reducing capacity (FRAP) assay. A central composite design (CCD) with four variables and five levels was employed for optimization of process parameters, and response surface plots were constructed in accordance with a second order polynomial model. Under optimal conditions of 3.0 h, 60.4 °C, 26.5 MPa and 89.3% ethanol, the highest yields were predicted to be 3.8 mg/g for total alkaloids, 0.5 mg/g for peimisine, 1.3 mg/g for peimine and 1.3 mg/g for peiminine, and the antioxidant capacity of extracts displayed EC50, DPPH value of 5.5 mg/mL, EC50, ABTS value of 0.3 mg/mL and FRAP value of 118.2 mg ascorbic acid equivalent (AAE)/100 g.

The technology of Supercritical Fluid Extraction is a new subject from Modern Chemicals Industries, which is one of the advanced Separation Technology. As for SCF(Supercritical Fluid), it is was that fluid on Critical Point(Pc, Tc) under Thermodynami..

SFE uses supercritical CO2, instead of organic solvents such as hexane and methylene chloride, to extract chemical compounds from a solid matrix (sometimes also from liquids). Near the critical point the density of a SCF is extremely sensitive to minor changes in temperature and pressure. Since the solvating power of a SCF is directly related to its density, selective extraction of the analyte of interest can be achieved by making slight changes in temperature and pressure and exploiting the differential solubility of analytes in the SCF. On the other hand, due to the higher diffusion coefficients in supercritical fluids, SFE is faster than liquid extraction. SFE is also a more efficient extraction method since the lower surface tension of supercritical fluids allows penetration into small pores of the solid matrix which are not accessible to liquids. ...

This document explains Method 3560, which uses supercritical fluids for the extraction of TRPHs from soils, sediments, fly ash, solid-phase extraction media, and other solid materials.. You may need a PDF reader to view some of the files on this page. See EPAs About PDF page to learn more. ...

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Summarized supercritical fluid property,supercritical fluid application and supercritical fluid extraction technique. Introduced the present situation that researched in the home and abroad,compendium supercritical fluid technique profit and defect and orientation which will be researched.

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SARMENTO, C. M. P.; FERREIRA, S. R. S. and HENSE, H.. Supercritical fluid extraction (SFE) of rice bran oil to obtain fractions enriched with tocopherols and tocotrienols. Braz. J. Chem. Eng. [online]. 2006, vol.23, n.2, pp.243-249. ISSN 0104-6632. http://dx.doi.org/10.1590/S0104-66322006000200012.. Parboiled rice bran oil was obtained with supercritical CO2 at temperatures and pressures varying from 25 to 60ºC and from 150 to 250 bar, respectively. This study was divided into two different parts: initially, the experiments were carried out with one separation step. In the second part, experiments were performed with two separators in series. The temperatures and the pressures of the first separator were 25 and 40ºC, and 100 and 150 bar. The second separator was maintained at 2ºC and 25bar. This procedure results in the precipitation of rice bran oil with different concentrations of tocols in the first and second separators. The extracts obtained were analyzed by HPLC to verify the presence ...

This publication offers an outline of simple rules of SFE in addition to in-depth studies of either on- and off-line SFE equipment. The online coupling of SFE with either chromatographic and spectroscopics suggestions has been the topic of loads of examine attempt and is handled intimately. more moderen advancements, corresponding to off-line SFE of sturdy and liquid matrices, are commencing to allure loads of curiosity, and the insurance of those components will turn out of specific price to the analytical chemist. The overseas crew of authors has illustrated those issues with many `state-of-the-art purposes, and every bankruptcy presents a accomplished record of references. For the comfort of the reader, an appendix which includes strain conversion scales and supercritical fluid carbon dioxide density tables looks on the finish of the e-book ...

March 30, 2015 Unified Chromatography The Swiss Knife of analytics Nexera UC: the next era of supercritical fluid extraction and chromatography / Combination of SFC and LC separation technologies with MS/MS detection / SFE/SFC/MS platform for quick and easy on-line sample extraction

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Determination of methylmercury in sediments using supercritical fluid extraction and gas chromatography coupled with microwave-induced plasma atomic emission spectrometry ...

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Reprinted from: Rochfort S, Isbel A, Ezernieks V, et al. Utilisation of Design of Experiments Approach to Optimise Supercritical Fluid Extraction of Medicinal Cannabis. Sci Rep. 2020;10(1):9124. doi:10.1038/s41598-020-66119-1. License: Creative Commons Attribution 4.0 International.. Run #1, with high flow rate (150 g/min), high pressure (300 bar), and a long extraction time (10 hours), dominated the chart in terms of yield for both cannabinoid recovery and extract weight. Flow rate was the most impactful factor overall, followed by time and then pressure. THC recovery depended more significantly on time compared to CBD recovery or weight.. There were unique CBD:THC ratios depending on extraction parameters. Runs #6 and #7 illustrate this point with similar extract weights but unique CBD:THC ratios. If the biomass were hemp, the study authors reason, this method may be optimised further so that low levels of THC could be removed.. The study did not account for lipids and other unwanted plant ...

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