Tetrasodium tris(bathophenanthroline disulfonate)ruthenium(II) (Na4Ru(bps)3) is a coordination compound containing a ruthenium center. In this form, it is the salt of a sulfonic acid. This compound is an extension of the well known phenanthroline series of coordination compounds. Ruthenium(II) tris(bathophenanthroline disulfonate), referring to the anionic fragment, is used as a protein dye in biochemistry for differentiating and detecting different proteins in laboratory settings.. In recent years, 2-D electrophoresis has been widely accepted as a standard procedure to separate complex protein mixtures in proteome studies (Proteomics). Protein visualisation by Ruthenium(II) tris(bathophenthroline disulfonate) has become a firmly established and widely used method in proteomic analysis [1][2][3][4][5][6][7][8][9][10][11][12][13][14][15][16] and a crucial step in gene expression profiling.. For protein detection, it is advantageous to use fluorescent labels containing chromophores which have ...
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The mononuclear metal complexes of the chelating bidentate 1,10-phenanthroline (phen) and 2,2-bipyridine (bipy) ligands are well known in the literature, and have been used in many fields. In the realm of coordination polymers, these complexes have been employed as coordination acceptor nodes for the construction of low dimensional polymer-based magnets exhibiting long-range magnetic ordering and spin crossover transitions. 1,10-Phenanthroline is of great interest in the field of supramolecular chemistry, because it can bring C-H···O or C-H···N hydrogen bonds and π-π stacking interactions (Liu et al., 2004 and Wang et al., 2003), which can effectively result in one-dimensional or two-dimensional networks. We report here the preparation and crystal structure of the title compound,[Cu(C9H7O2)2(C12H8N2)].. The asymmetric unit contains a half CuII cation, a half phen ligand and one cinnamic ligand (L-: C6H5-CH=CH-COO-). The CuII atom lies on a twofold rotation axis. In the complex, two ...
Attempts to co-crystallise the nucleobases adenine, thymine, guanine, and cytosine with 1,10-phenanthroline by ball milling and solvent evaporation methods are described. A 1 : 1 co-crystal of cytosine and 1,10-phenanthroline can be obtained by grinding or by solvent evaporation. The structure contains two c
Recovered papers contain several chromophores, such as wood lignin and dyes. These have to be eliminated during paper recycling in order to produce white paper. Hydrogen peroxide under alkaline conditions is generally used to decolorize lignin, but its effect on dyes is limited. Copper(II)-phenanthroline (Cu-Phen) complexes can activate the oxidation of lignin by hydrogen peroxide. Hydrogen peroxide may also be activated during recycled fiber bleaching, thus enhancing its color-stripping efficiency towards unoxidizable azo dyes. The purpose of this paper was to determine the effect of Cu-Phen complexes on a model azo dye, Direct Red 81 (DR81), in aqueous solution. Different Cu-Phen solutions (with different initial Cu:Phen molar ratios) were prepared and mixed with the dye at different pHs. The geochemical computer program PHREEQC allowed precise calculation of the theoretical distribution between different possible coordinates (CuPhenOH+, Cu(Phen)22+, CuPhen(OH)2, Cu(Phen)32+, etc.) depending on pH and
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To explore the binding properties of [Ru(phen)(2)dppz](2+) complex (phen = l,10-phenanthroline, dppz = dipyrido[3,2-a:2,3-c]phenazine) in a sequence-specific manner in DNA duplex. it was tethered through the dppz ligand to a central position as well as. ...
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Chemical Reviews, Vol. 112 (3), p. 1344-1462. eISSN 1520-6890. Article.. Chelucci, Giorgio Adolfo and Thummel, Randolph P. (2002) Chiral 2,2-Bipyridines, 1,10-Phenanthrolines, and 2,2:6,2-Terpyridines: syntheses and applications in asymmetric homogeneous catalysis. ...
Elemey="Table that containBceSe= true;" class="popup" id="cellVorder_view);Popup">order_view; if (nb_number of== 0) {alert(Px.phen=Search&dex.php?acti thos=Search&ncoord=4};td (authorsHelpP;">Elemey="Table that containPactirn= true;" class="popup" id="cellVorder_view);Popup">order_view; if (nb_number of== 0 ,, nb_number of>= 4) {alert(Px.phen=Search1dimenbold; fon_ranPactirn dras=Search&ncoord=4};td (authorsHelpP;">Elemey="Table that containXDS">XDS = true;" class="popup" id="cellVorder_view);Popup">order_view; if (nb_number of== 0 ,, nb_number of>= 5) {alert(Px.phen=Search1dime4bold; fon_ranVRML dras=Search&ncoord=4};td (authorsHelpP;">Elemey="Table that containJmo = true;" class="popup"openJmo (jmo =SePopup">ojmo ; if (nb_number of== 0 ,, nb_number of>= 5) {alert(Px.phen=Search1dime4bold; fon_ranJmo dras=Search&ncoord=4};td ("="17"se;/ alse;/ body= uteHelpPo ut name="authors" sb">Aut="0 ...
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Using the sequential injection analysis with the spectrophotometric detector, the kinetic method for the determination of cysteine was developed and validated. The kinetic method is based on redox reaction where cysteine as a reductant, reduces green copper(II) neocuproine complex to copper(I) neocuproine complex. The formated yellow-orange copper(I) neocuproine complex shows an absorption maximum at wavelength of 458 nm. The optimum parameters of the flow system were determined by a univariate method and as a result the calibration curve was constructed. Linearity was achieved for the concentration range from 6.0  10 7 mol L 1 to 8.0  10 5 mol L 1 and it was described with the equation y = 3690.4 x + 0.0019 and correlation coefficient R 2 = 0.9997. The calculated limit of detection is 1.8  10 -7 mol L -1 and the limit of quantification is 6.0  10 7 mol L 1 . The influence of foreign substances commonly found in the composition of the pharmaceutical preparations was ...
Research on chemotherapeutics for lung cancer is crucial for designing a new therapeutic strategy against malignant lung tumors. Although radiotherapy and chemotherapy, which are not selective for cancer cells and exert toxic effects on healthy cells, have a limited advantage, they are the primary treatment modalities for non-small lung cancer. In addition to cytotoxicity, resistance of chemotherapeutics results in failure of treatment. This is why it is of utmost importance to focus on the creation of new chemotherapeutics without toxicity for the successful treatment and improved survival of cancer patients. New gold(III) and Pt(II) compounds were synthesized with a heterocyclic ligand using 2-phenylimidazo[4,5-f][1,10]phenanthroline as a ligand and bis-1,4-di[([1,10] phenanthroline-5-il)amino]-2-buten as a bridge molecule. The characterization of the compounds was carried out using a variety of spectroscopic methods (H-1 NMR, IR, MS, and elemental analysis). Their antiproliferative, ...
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o-Phenanthroline monohydrochloride monohydrate 3829-86-5 NMR spectrum, o-Phenanthroline monohydrochloride monohydrate H-NMR spectral analysis, o-Phenanthroline monohydrochloride monohydrate C-NMR spectral analysis ect.
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A palladium(II)-catalyzed arylation of a γ-C(sp³)-H bond of protected amino acid is explored. The monoarylation is promoted by the commercially available, inexpensive phenanthroline ligand, and toxic silver salt is replaced by earth-abundant Mn(III)acetate. Subsequently, a hitherto unknown unsymmetrical diarylation at the γ-position is accomplished under the modified reaction conditions. Ligands h ...
Protein levels regressed against four cytotoxicity phenotypes using fixed effect or mixed effect models representing the three biological replicates.We analyzed
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1, 10 copper phenanthroline assay is a frequently used assay to examine the pro-oxidative activity of extracts against DNA [26]. On addition of reagents and subsequent incubation, a complex called bis (1, 10 - phenanthroline copper) is formed which links to DNA and breaks down its strand; hydroxyl radical generation is primarily implicated in DNA damage [39]. However, if the cuprous ions are bound, DNA degradation does not occur. When reducing agent ascorbic acid (which is a proven pro-oxidant at higher concentration [40]) is added to the complex, Cu(II) in the complex gets converted to Cu(I) and hence, there is additional production of hydroxyl radicals that breaks down DNA into TBARS (Thiobarbituric Acid Reactive Substance). Hence, the level of TBARS formed in different extracts/fractions can indirectly reveal the quantity of hydroxyl radicals generated and give an estimation of the pro-oxidant or anti-oxidant activity of the extract/fractions at varying concentration. ROS (Reactive Oxygen ...
Free radicals contribute to Type 1 diabetes (T1D) autoimmune responses. We recently demonstrated that superoxide-deficient CD4 T cells exhibited increased effector responses and diabetogenicity, but the redox-dependent mechanism(s) mediating T cell activation were unclear. We hypothesized that during T1D progression, CD4 T cells with a reduced cell surface state would exhibit a concomitant increase in pro-inflammatory cytokine and chemokine responses. To test this, alexa fluor 647-conjugated maleimide (ALM)-labeling of cell surface reduced thiols on diabetogenic mouse and human CD4 T cells was performed. We observed an increase in ALM percentage and gMFI from peripheral Non-obese diabetic (NOD) mouse CD4 T cells during progression to overt diabetes. Cognate autoantigen stimulation elicited a 2- and 20-fold increase in CD4 ALM T cell percentage and gMFI, respectively. In addition to serving as a T cell activation marker, ALM gMFI of reduced CD4 T cell surface thiols was enhanced (1.2-fold) with ...
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Makrlík Emanuel, Vaňura Petr, Selucký Pavel, Babain Vasily, Alyapyshev Mikhail, Darin Dmitriy: Highly Efficient Solvent Extraction of Americium and Europium by Using Hydrogen Dicarbollylcobaltate and N,N′-Diethyl-N,N′-bis(4-ethylphenyl)-1,10-phenanthroline-2,9-dicarboxamide. J Solution Chem 2017, 46, 1475. ,https://doi.org/10.1007/s10953-017-0651-6 ...
Abstract: Preorganization has been shown to be an important concept in inorganic chemistry. Preorganization increases the thermodynamic stability of complexes and metal ion selectivity of ligands. A ligand is more highly preorganized the more nearly it is constrained as the free ligand to be in the conformation required to complex the metal ion. The ligand 2,9-bis(hydroxymethyl)-1,10-phenanthroline (PDALC) was used to study the effects of preorganization and effects of addition of neutral oxygen donor atoms on the thermodynamic complex stability. The rigid extended aromatic backbone of PDALC should lead to unprecedented levels of preorganization for a non-macrocyclic ligand. PDALC was synthesized and characterized using NMR and IR analysis. UV/Vis spectrophotometry was used in titrations to determine protonation constants of the free ligand and its formation constants with metal ions. These were obtained by plotting absorbance, corrected for dilution caused by addition of acid or base during the ...
The novel N,N,O-tridentate phenanthroline ligand (BinThro) bearing an axially chiral binaphthyl backbone prepared from BINOL was found to be an effective chiral catalyst for enantioselective addition of diethylzinc to aromatic aldehydes with high enantioselectivity (up to 95% ee).
The amino acids complexes of [Pt(phen)(AA)]NO3·xH2O and [Pd(phen)(AA)]NO3·xH2O have been prepared by the interaction of palladium and platinum complexes, [Pt(phen)Cl2] and [Pd(phen)Cl2] with salts of amino acids in methanol and characterized by 1H NMR and IR spectroscopy which confirmed the formation of a very large variety of compounds with ligand in a simple way (bidentate). All of these new compounds have been isolated and tested for cytotoxicity on Molt-4, a human leukaemia cell line. The IC50 values of [Pt(phen)(Pro)]Cl·2H2O and [Pd(phen)(Asp)]Cl·1.5H2O are 9.8 and 7.31 μM, respectively, exhibiting a significant activity which is close to cis-[PtCl2(NH3)2]. (C) 2000 Elsevier Science S.A ...
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The mitochondrial ADP/ATP carrier imports ADP from the cytosol and exports ATP from the mitochondrial matrix. The carrier cycles by an unresolved mechanism between the cytoplasmic state, in which the carrier accepts ADP from the cytoplasm, and the matrix state, in which it accepts ATP from the mitochondrial matrix. Here we present the structures of the yeast ADP/ATP carriers Aac2p and Aac3p in the cytoplasmic state. The carriers have three domains and are closed at the matrix side by three interdomain salt-bridge interactions, one of which is braced by a glutamine residue. Glutamine braces are conserved in mitochondrial carriers and contribute to an energy barrier, preventing the conversion to the matrix state unless substrate binding occurs. At the cytoplasmic side a second salt-bridge network forms during the transport cycle, as demonstrated by functional analysis of mutants with charge-reversed networks. Analyses of the domain structures and properties of the interdomain interfaces indicate ...
Page contains details about 9,10-phenanthroline quinone/multi-walled carbon nanotubes-modified glassy carbon . It has composition images, properties, Characterization methods, synthesis, applications and reference articles : nano.nature.com
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A new dinuclear RuII polypyridyl complex, [(bpy)2Ru(H2bpip)Ru(bpy)2]4+ (RuH2bpip, bpy=2,2‐bipyridine, H2bpip=2,6‐pyridyl(imidazo[4,5‐f][1,10]phenanthroline ...
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