Triflic acid is a superacid, and it is the strongest Bronstedt acid available on a commercial scale. Many organic synthesis reactions (alkylation, esterification, isomerization, etherification, acylation, ethoxylation, cationic rearrangement, cyclization, etc.) and cationic polymerization use it as an anacidic catalyst.. Key Trends in Global Triflic Acid Market. Higher Demand in Pharmaceutical Industries. It is used to produce a variety of drug groups in the pharmaceutical industry, including nucleosides, antibiotics, hormones, proteins, and glycosides, and this is one of the primary factors driving the use of triflic acid. Vitamin synthesis, silicon rubber alteration, and catalyst isomerization and alkylation are some of its other uses. Triflic acids production is rapidly increasing as a result of its widespread use in the pharmaceutical and chemical industries. Over the forecast period, the expanding application spectrum of silicon rubber is expected to provide numerous growth ...
Triflic acid is a superacid, and it is the strongest Bronstedt acid available on a commercial scale. Many organic synthesis reactions (alkylation, esterification, isomerization, etherification, acylation, ethoxylation, cationic rearrangement, cyclization, etc.) and cationic polymerization use it as an anacidic catalyst.. Key Trends in Global Triflic Acid Market. Higher Demand in Pharmaceutical Industries. It is used to produce a variety of drug groups in the pharmaceutical industry, including nucleosides, antibiotics, hormones, proteins, and glycosides, and this is one of the primary factors driving the use of triflic acid. Vitamin synthesis, silicon rubber alteration, and catalyst isomerization and alkylation are some of its other uses. Triflic acids production is rapidly increasing as a result of its widespread use in the pharmaceutical and chemical industries. Over the forecast period, the expanding application spectrum of silicon rubber is expected to provide numerous growth ...
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TY - JOUR. T1 - Trifluoromethanesulfonic acid-catalyzed tandem semi-pinacol rearrangement/alkyne-aldehyde metathesis reaction of arylpropagylsulfonamide- tethered 2,3-epoxycyclohexan-1-ols to spiropiperidines. AU - Lin, Ming Nan. AU - Wu, Shih Hui. AU - Yeh, Ming-Chang P.. PY - 2011/12/1. Y1 - 2011/12/1. N2 - A simple and efficient trifluoromethanesulfonic acid-catalyzed cycloisomerization of arylpropagylsulfonamide-tethered 2,3-epoxycyclohexan-1-ols is described. The cyclization proceeds via tandem semi-pinacol rearrangement/alkyne-aldehyde metathesis to afford spiropiperidines under mild reaction conditions.. AB - A simple and efficient trifluoromethanesulfonic acid-catalyzed cycloisomerization of arylpropagylsulfonamide-tethered 2,3-epoxycyclohexan-1-ols is described. The cyclization proceeds via tandem semi-pinacol rearrangement/alkyne-aldehyde metathesis to afford spiropiperidines under mild reaction conditions.. KW - alkyne/aldehyde metathesis. KW - semi-pinacol rearrangement. KW - ...
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Methyl methanethiosulphonate was used to produce a modification of the essential thiol group in lactate dehydrogenase which leaves the enzyme catalytically active. Methyl methanethiosulphonate produced a progressive inhibition of enzyme activity, with 2mM-pyruvate and 0.14mM-NADH as substrates, which ceased once the enzyme had lost 70-90% of its activity. In contrast, with 10mM-lactate and 0.4mM-NAD+ as substrates the enzyme was virtually completely inhibited. The observed inhibition was critically dependent on the chosen substrate concentration, since methanethiolation with methyl methanethiosulphonate resulted in a large decrease in affinity for pyruvate. At 0.14mM-NADH, methanethiolation increased the apparent KmPyr from from 40micronM for the control enzyme to 12mM for the modified enzyme. Steady-state kinetics showed that there was not a statistically significant change in either KmNADH or KsNADH. At saturating NADH and pyruvate concentrations, the Vmax. was virtually unaffected for the ...
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0023]The term allergic inflammatory diseases, as used herein, refers to non-specific inflammatory diseases caused by a variety of allergens, and includes allergic rhinitis, asthma, allergic conjunctivitis, allergic dermatitis, atopic dermatitis, contact dermatitis, urticaria, anaphylaxis, insect allergy, food allergy, and drug allergy. The preventive and therapeutic efficacy of the N-hydroxy-4-{5-[4-(5-isopropyl-2-methyl-1,3-thiazol-4-yl)phenoxy]pentoxy} benzamidine compound on allergic inflammatory diseases was confirmed in a mouse model of asthma which was induced by chronic exposure to ovalbumin. The benzamidine compound was administered for a period of 18 days, starting on the day of immunization with ovalbumin. 15 days after immunization, experimental animals were challenged with ovalbumin, and sacrificed three days later to investigate lung weight, changes in the cellular profile of bronchoalvelar lavage fluid and peripheral blood samples, and histopathological changes in lung tissue. ...
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TY - JOUR. T1 - Immunoregulatory activity in adult rat testicular interstitial fluid: relationship with intratesticular CD8+ lymphocytes following treatment with ethane dimethane sulfonate and testosterone implants. AU - Hedger, Mark. AU - Wang, Jian. AU - Lan, Hui Y. AU - Atkins, Robert C. AU - Wreford, Nigel G. PY - 1998. Y1 - 1998. M3 - Article. SP - 935. EP - 942. JO - Biology of Reproduction. JF - Biology of Reproduction. SN - 0006-3363. ER - ...
A deglycosylated derivative of tomato (Lycopersicon esculentum) lectin was prepared with the use of trifluoromethanesulphonic acid. Its properties were generally similar to those of the native lectin, but differences were evident in terms of relative agglutinating activity towards sheep, (untreated) human and trypsin-treated human erythrocytes. The two forms of tomato lectin were used in conjunction with a battery of specific antisera to investigate structural relatedness among solanaceous lectins. Immunological cross-reactivity between tomato, potato and Datura lectins depends on the integrity of the glycosylated region of those lectins; that between Datura lectin and other seed lectins, however, has a separate structural basis.. ...
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Direct acidolysis to monomers. Having demonstrated that our organosolv lignins could be converted into native-like lignins potentially suitable for further valorisation using known methods,9,10,82 we considered if direct selective depolymerisation to aromatic chemicals may be possible. Given the demonstrated reversibility of the α-etherification under acidic conditions we investigated the use of a triflic acid mediated lignin depolymerisation method recently reported by Barta and de Vries et al.25,83 In this process triflic acid first promotes a retro-Prins reaction of the β-O-4 linkages, likely via a benzylic cation, to give an intermediate enol ether which then undergoes hydrolysis and in situ acetal formation to give P1-P3 (see Scheme S1† for more details). Initially, using Bi(OTf)3 as a convenient alternative to triflic acid,84 we found that our lignins were efficiently depolymerised to give the expected acetals in 1,4-dioxane in moderate to good yields without any need to carry out the ...
Eatons reagent (7.7 wt% phosphorus pentoxide solution in methanesulfonic acid) is used as an alternative to polyphosphoric acid in chemical synthesis to promote acylation reactions. Eaton, P. E.; Carlson, G. R.; Lee, J. T. (1973). Phosphorus pentoxide-methanesulfonic acid. Convenient alternative to polyphosphoric acid. J. Org. Chem. 38 (23): 4071. doi:10.1021/jo00987a028 ...
Chemical Equation Presented) Cyclization reactions involving cyanoacetylated bisindoles have been studied, providing access to various novel cyclohepta[2,1-b:3,4-b′]diindole derivatives as well as some related fused pentacyclic systems. Treatment of 3-cyanoacetyl-2,3′-diindolylmethane with methanesulfonic acid gave 6-(cyanomethyl)indolo[3,2-b]carbazole in a good yield.. ...
The four Ugi products ([http://www.ourexperiment.org/racemic_pzq/4029/Preparation_of_the_PZQ_peptide_acetal_Ugiintermediate_KAB52.html KAB5-2], [http://www.ourexperiment.org/racemic_pzq/5642/Preparation_of_the_dimethoxy_Ugiintermediate_MNR85.html MNR8-5], [http://www.ourexperiment.org/racemic_pzq/1555/Preparation_of_the_Nbenzoylprotected_Ugiintermediate_MW511.html MW51-1], [http://www.ourexperiment.org/racemic_pzq/4011/Preparation_of_the_dimethoxy_Ugiintermediate_MNR102.html MNR10-2]) were subjected to varying loading levels of methanesulfonic acid to study its effect on the cyclisation. Initially the reactions were carried out in neat acid using 100 equivalents. The reaction to afford PZQ ([http://www.ourexperiment.org/racemic_pzq/2443/Acidmediated_PictetSpengler_of_MW29_to_give_racPZQ_MNR131.html MNR13-1]) was the only one that did not give clean conversion to desired product at room temperature after 1 hour but all starting material was consumed. It was however found that increasing the ...
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149194-25-2 - ZMDLBLZFZSHVLH-UHFFFAOYSA-N - 1-Acetyl-1,2-bis(methylsulfonyl)-2-(2-chloroethyl)hydrazine - Similar structures search, synonyms, formulas, resource links, and other chemical information.
You are viewing an interactive 3D depiction of the molecule n-{2-benzyl-4-[(methylsulfonyl)carbamoyl]phenyl}-6-(cyclohexylmethyl)-2-pyridinecarboxamide (C28H31N3O4S) from the PQR.
2-(Methylsulfonyl)-5-(tributylstannyl)pyrimidine; CAS Number: 122476-85-1; find Synthonix Corporation-SY3371478447 MSDS, related peer-reviewed papers, technical documents, similar products & more at Sigma-Aldrich
2-Bromo-4-(methylsulfonyl)pyridine; CAS Number: 1193244-93-7; find Synthonix Corporation-SY3H3D67735E MSDS, related peer-reviewed papers, technical documents, similar products & more at Sigma-Aldrich