Journal of Applied CrystallographyInternational Union of CrystaSpectroscopy2023Tomography2020Fundamentals of CrystallographyElectron diffractionMacromolecular crystallographyIUCrPXRDNanoDeterminationMethodsDiffractometerLaboratoryDetectorScatteringCoherentExperimentsPatternsNeutron powderChemistryBragg'sRefinementsMineralogy2022Small moleculesInorganic materialsAnalyticalHigh-throughputTransformationsBeamDataTechniquesAnalysisCapillariesBasicsFingerprintProteinReciprocal spaceWavelengthCrystalline solidSingleRadiationMaterialsBeamlineAtomicOptics
Journal of Applied Crystallography3
- Journal of Applied Crystallography (2023) 56 (1): 263. (geoscienceworld.org)
- Journal of Applied Crystallography 2015 , 48 , 79-84. (mpg.de)
- Journal of Applied Crystallography , 53 , 1169-1180. (uni-luebeck.de)
International Union of Crysta1
- The International Union of Crystallography is therefore pleased to announce the launch of a new section of IUCrJ dedicated to electron crystallography. (iucr.org)
Spectroscopy5
- Formed in July of 2007, to support the research endeavors at Michigan State University, with resources for Single Crystal X-ray Diffraction (SCXRD), Powder X-ray Diffraction (PWXRD) and X-ray Fluorescence Spectroscopy (XRF). (msu.edu)
- We have piloted data search through heterogeneous data sources from a single interface across samples and experiments for Inner Shell Spectroscopy (ISS) and X-ray Powder Diffraction (XPD). (bnl.gov)
- of these as possible using optical crystallography, X-ray diffraction, and infrared spectroscopy. (irkutsk.ru)
- His research centres on the applications and development of high-resolution electron microscope techniques, in particular scanning transmission electron microscopy (STEM) including 4D STEM diffraction-imaging techniques, Z -contrast imaging, electron energy-loss spectroscopy and applications of spherical aberration correctors. (iucr.org)
- His technique development work includes ptychography, quantification of diffraction and image data, methods for the three-dimensional imaging and spectroscopy of materials using optical sectioning, and methods to allow high-resolution imaging and spectroscopy of radiation sensitive materials. (iucr.org)
20233
- Powder Diffraction (2023) 38 (3): 194. (geoscienceworld.org)
- Powder Diffraction (2023) 38 (1): 37. (geoscienceworld.org)
- Powder Diffraction (2023) 38 (2): 145. (geoscienceworld.org)
Tomography1
- Louisa Meshi (Ben-Gurion University of the Negev, Beer-Sheva, Israel) specializes on structure solution of complex intermetallics applying precession electron diffraction (PED), convergent beam electron diffraction (CBED) and 3D electron diffraction tomography methods. (iucr.org)
20202
- 2020 - currently, Technician-Geology - Experimental Mineralogy, Institute of Mineralogy and Crystallography "Acad. (bas.bg)
- Hoffmann, F. (2020): Introduction to Crystallography. (uni-bremen.de)
Fundamentals of Crystallography2
- Fundamentals of Crystallography: the theory behind crystal structure solution. (iucr.org)
- Giacovazzo, C. (2011): Fundamentals of crystallography. (uni-bremen.de)
Electron diffraction6
- Powder diffraction is a scientific technique using X-ray, neutron, or electron diffraction on powder or microcrystalline samples for structural characterization of materials. (wikipedia.org)
- Powder electron diffraction is more complex due to dynamical diffraction and is not discussed further herein. (wikipedia.org)
- Mauro Gemmi (Istituto Italiano di Tecnologia, Pontedera, Italy) has worked in several electron microscopy labs in Europe (Stockholm University, Milan University, Institut Néel Grenoble) becoming an expert in the application of electron diffraction to structure solution problems. (iucr.org)
- He has been among the first to extensively use precession electron diffraction for solving crystal structures. (iucr.org)
- His main research goal has been to apply electron diffraction to structural problems in any field of crystallography. (iucr.org)
- In relation to structure characterization methods, Junliang and his co-workers have developed rotation electron diffraction which pushed the size limitation for single-crystal diffraction to tens of nanometres. (iucr.org)
Macromolecular crystallography1
- The Life Sciences Collaborative Access Team (LS-CAT) formed in 2002 provides macromolecular crystallography resources for those with a need to determine the structure of proteins. (msu.edu)
IUCr1
- Recent years have seen the rapid development and expansion of electron crystallography, much of it highlighted at the IUCr Congress in Prague last year. (iucr.org)
PXRD1
- Powder X-ray diffraction (PXRD) operates under the assumption that the sample is randomly arranged. (wikipedia.org)
Nano2
- In her laboratory, structure solution of these phases (appearing as nano-sized precipitates in metallic matrices) is combined with characterization of line and planar crystalline defects (using various electron imaging and diffraction methods), aiming at development of structural materials of tomorrow. (iucr.org)
- The development of new methods is central to this work, particularly using emerging technologies in cryo-electron microscopy, nano and coherent X-ray diffraction, and macromolecular design. (iucr.org)
Determination4
- The X-ray Crystallography Center (XCC) offers high-level instrumentation and expertise in sample analysis and crystal structure determination from X-ray diffraction data. (fsu.edu)
- t -AlF 3 - crystal structure determination from X-ray powder diffraction data - a new MX 3 corner-sharing octahedra 3D network," J. Solid State Chem . (crystallography.net)
- Small molecule crystallography uses X-ray diffraction in the determination and study of the three dimensional structure of a material at the atomic and molecular scale. (excillum.com)
- Easy and rapid access to brilliant synchrotron X-rays is a vital ingredient for three-dimensional structure determination of drug targets through macromolecular X-ray crystallography. (lu.se)
Methods11
- Relative to other methods of analysis, powder diffraction allows for rapid, non-destructive analysis of multi-component mixtures without the need for extensive sample preparation. (wikipedia.org)
- Beyond the excellent instrumental capabilities, the XCC also offers expertise and user training in X-ray methods provided by the facility director, Dr. Xinsong Lin. (fsu.edu)
- The nanoprobe experiment is optimized for ptychographic methods with resolution down to 10 nm whereas the microprobe experiment is a more versatile setup for fast scanning X-ray microscopy using KB optics providing 300 nm focus size. (wayforlight.eu)
- Traditional X-ray Diffraction methods employed for quenching inspection use low-energy monochromatic X-rays that cannot penetrate the sample volume. (advacam.com)
- X-ray diffraction methods and up-to-date methods for X-ray diffraction data analysis will be understood in detail and the students will be able to apply the latter. (uni-bremen.de)
- knowledge in crystallography will be the prerequisitefor the understanding of 3-dimensional crystal structures - knowledge in symmetry relationships and laws will be the prerequisite for understanding crystal properties - training in X-ray diffraction methods will enable students to identify minerals and crystalline compounds, and to determine atomic positions in crystals. (uni-bremen.de)
- Junliang Sun (Peking University, Beijing, China) works mainly on the development of structure characterization methods (electron crystallography and powder X-ray diffraction) and the synthesis of inorganic materials. (iucr.org)
- Browse our X-ray crystallography library to learn more about the methods we use. (bath.ac.uk)
- Methods based on scattering and diffraction utilize that radiation can "change direction" when interacting with an object. (excillum.com)
- Spectroscopic X-ray methods are based on detecting X-ray energy spectra. (excillum.com)
- The MATFab Facility is seeking an Assistant Research Scientist/Engineer to: manage, perform experiments, and develop methods of analysis of powder and single-crystal X-ray data and perform refinements of crystal structures. (blogspot.com)
Diffractometer7
- An instrument dedicated to performing such powder measurements is called a powder diffractometer. (wikipedia.org)
- The X-Ray Lab holds a Rigaku powder x-ray diffractometer, purchased through a joint chemistry-physics grant from the National Science Foundation. (oberlin.edu)
- The XCC facility houses three newly acquired Rigaku instruments: a Synergy-S four-circle single-crystal diffractometer with a dual-source Cu/Mo radiation, a SmartLab powder diffractometer, and a MiniFlex benchtop powder diffractometer (both with Cu sources). (fsu.edu)
- In addition to these instruments, facility users also enjoy access to a dual-source (Cu/Mo) Panalytical X'Pert Pro powder diffractometer, and a Panalytical Epsilon X-ray fluorescence analyzer. (fsu.edu)
- New sixth generation MiniFlex benchtop X-ray diffractometer is a multipurpose powder diffraction analytical instrument that can determine: crystalline phase identification (phase ID) and quantification, percent (%) crystallinity, crystallite size and strain, lattice parameter refinement, Rietveld refinement, and molecular structure. (fsu.edu)
- The XtaLAB Synergy-S single crystal X-ray diffractometer comes with kappa goniometer that incorporates fast motor speeds and a unique telescopic two-theta arm to provide total flexibility for the diffraction experiment. (fsu.edu)
- Once in Delft, she was again the initiator of several big instrumentation projects, such as the neutron powder diffractometer PEARL or the multipurpose instrument LARMOR , a Dutch-UK collaboration, which is being built at the UK neutron source ISIS and is supported by a NWO-Groot grant. (tudelft.nl)
Laboratory3
- Weidenthaler, C. An in situ powder diffraction cell for high-pressure hydrogenation experiments using laboratory X-ray diffractometers. (mpg.de)
- The X-Ray Diffraction laboratory. (bath.ac.uk)
- This imaging technique is since many years performed at synchrotrons, but in recent decades the optics-based X-ray microscope based on laboratory sources are commercially available. (excillum.com)
Detector7
- When the scattered radiation is collected on a flat plate detector, the rotational averaging leads to smooth diffraction rings around the beam axis, rather than the discrete Laue spots observed in single crystal diffraction. (wikipedia.org)
- A report on the characterization, calibration and performances of the MYTHEN photon-counting silicon microstrip detector at the powder diffraction station at the Swiss Light Source is given. (scienceopen.com)
- The MYTHEN single-photon-counting silicon microstrip detector has been developed at the Swiss Light Source for time-resolved powder diffraction experiments. (scienceopen.com)
- An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. (scienceopen.com)
- Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high-resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. (scienceopen.com)
- D/teX Ultra 250 1D detector accelerates powder diffraction by a factor of 250 in speed and provides adjustable energy resolution of approximately 20% or 4% depending on sample type. (fsu.edu)
- Our equipment: RIGAKU Oxford Diffraction SuperNova, Dual source (Mo and Cu, 0.71073 Å and 1.5418 Å) detector EosS2 and RIGAKU Oxford Diffraction Xcalibur (Mo) detector EosS2, with the data processing software CrysAlisPro. (bath.ac.uk)
Scattering5
- The angle between the beam axis and the ring is called the scattering angle and in X-ray crystallography always denoted as 2θ (in scattering of visible light the convention is usually to call it θ). (wikipedia.org)
- Powder diffraction data are usually presented as a diffractogram in which the diffracted intensity, I, is shown as a function either of the scattering angle 2θ or as a function of the scattering vector length q. (wikipedia.org)
- On the basis of the presence of Bragg peaks in the recorded small-angle X-ray scattering profiles, it is possible to assess within seconds whether a cell culture contains microcrystals, even in a small percentage of cells. (uni-luebeck.de)
- Small Angle X-ray Scattering is used to study the structure of materials in the 1 nm to ~200 nm range. (excillum.com)
- Small-angle X-ray scattering can also be used as a complementary technique to study proteins in room temperature. (lu.se)
Coherent1
- And the PyNX software suite, initially released in 2018, processes coherent X-ray imaging data. (minatec.org)
Experiments2
Patterns1
- The Fox software Vincent developed in the 2000s, which uses powder diffraction patterns to determine the structure of crystals, is still relevant today. (minatec.org)
Neutron powder1
- The most common type of powder diffraction is with x-rays, the focus of this article although some aspects of neutron powder diffraction are mentioned. (wikipedia.org)
Chemistry3
- The equipment and related crystallography software are used in inorganic chemistry, intermediate and advanced physics labs, and in mineralogy as well as in a variety of student-faculty research projects. (oberlin.edu)
- I want to get the latest chemistry news from C&EN in my inbox every week. (acs.org)
- The Summer School is intended for graduate students, PhD students, and young scientists active in solid state research (chemistry, physics), geo-sciences, crystallography, and materials science. (dgk-home.de)
Bragg's1
- If the atoms are arranged symmetrically with a separation distance d, these waves will interfere constructively only where the path-length difference 2d sin θ is equal to an integer multiple of the wavelength, producing a diffraction maximum in accordance with Bragg's law. (wikipedia.org)
Refinements2
- The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage. (scienceopen.com)
- Four workshop sessions led by N. Bhuvanesh, C. Campana (both on powder diffraction), P. Mueller (difficult refinements) and G. Sheldrick (TWINABS) allowed the participants to fine-tune their skills. (iucr.org)
Mineralogy1
- Institute of Mineralogy and Crystallography "Acad. (bas.bg)
20221
- Powder Diffraction (2022) 37 (2): 98. (geoscienceworld.org)
Small molecules1
- Provides 3-dimensional structure of small molecules in solid crystals via X-ray crystallography. (ucla.edu)
Inorganic materials1
- Facility users also have access to the Cambridge Crystal Structure Database (CCSD) for organic and organometallic compounds and to the Inorganic Crystal Structure Database (ICSD) for inorganic materials, as well as to the extensive Powder Diffraction File (PDF) database. (fsu.edu)
Analytical2
- Analytical services provided using x-ray diffraction. (msu.edu)
- X-ray diffraction is an analytical method based on the inspection of the crystalline structure of samples. (advacam.com)
High-throughput1
- MAX IV offers state-of-the-art instruments and world-class tools for crystallography as well as high-throughput screening techniques. (lu.se)
Transformations1
- On the second day G. Sheldrick led a discussion of future developments in SHELX, S. Lindeman made a strong case for using CuKα radiation, L. Falvello and B. Foxman spoke about solid state transformations, J. Reibenspies described powder diffraction applications, H. Hope illustrated a cryocrystallography set-up for use in the 5-20 K range, and G. Yap and L. Dahl delivered spirited talks on teaching X-ray crystallography. (iucr.org)
Beam3
- It allows one to trade-off coherence properties of the beam with the intensity falling onto the entrance slits of the scanning X-ray microscope. (wayforlight.eu)
- A powerful Kirkpatick-Baez (KB) mirror system can be used for X-ray beam focussing with spot sizes down to about 300 nm x 300 nm in air with a free working distance of 18 cm between KB optics enclosure and the focal plane. (wayforlight.eu)
- The XRD measurements performed in transmission mode with polychromatic X-ray beam of 160 kVp. (advacam.com)
Data5
- Ltd, the partners of the International Centre for Diffraction Data in India. (unigoa.ac.in)
- Finally, thanks to technological breakthroughs at the European Synchrotron Research Facility in France, Nelson managed to collect single-crystal X-ray diffraction data from her tiny crystals. (acs.org)
- Our equipment: STOE STADI P double setup with Mythen detectors using Cu-Kα1 radiation, with the data processing software WinXPOW, with two independent working areas: one for transmission or Debey-Scherrer geometry (for tiny amounts of powders wedged in between foils or powder samples in capillaries), the other one in flatplate or Bragg-Brentano geometry (for thin films or coarse materials). (bath.ac.uk)
- Powder diffraction data usually fall under the poor resolution/data quality category and as such additional symmetry restraints using symmetry_obey_0_to_1 can sharpen electron densities. (durham.ac.uk)
- Example CF-ALVO4.INP demonstrates the use of the tangent formula on powder data. (durham.ac.uk)
Techniques4
- Powder diffraction stands in contrast to single crystal diffraction techniques, which work best with a single, well-ordered crystal. (wikipedia.org)
- Because the crystals were far too small to analyze by conventional single-crystal X-ray diffraction techniques, Nelson threw herself into determining their structure using powder X-ray diffraction of crystal aggregates. (acs.org)
- Equipped for characterization of polycrystalline solid materials using powder and thin film diffraction techniques. (ucla.edu)
- Read about some X-ray techniques, and learn about their potentials and the requirements on the equipment. (excillum.com)
Analysis1
- Powder XRD is mainly used for structural analysis of microcrystalline solid materials or powder samples. (excillum.com)
Capillaries1
- Several sample holders can be used for powders or in capillaries, some with Anton Paar temperature stages. (fsu.edu)
Basics1
- Hammond, C. (2009): The Basics of Crystallography and Diffraction. (uni-bremen.de)
Fingerprint1
- The powder pattern fingerprint is so accurate that predictions not much better than 1% on the (real) cell parameters will not necessarily be disclosed. (crystallography.net)
Protein2
- LS-CAT provides access to state-of-the-art x-ray diffraction facilities at Argonne National Laboratory's Advanced Photon Source where extremely intense beams of x-rays are focused using both mirrors and beryllium lenses onto tiny protein crystals. (msu.edu)
- Protein crystallographers rely on the brightest X-ray sources to combat the issues of air sensitivity, small crystals, low diffraction and densely packed reflections. (excillum.com)
Reciprocal space1
- This is because orientational averaging causes the three-dimensional reciprocal space that is studied in single crystal diffraction to be projected onto a single dimension. (wikipedia.org)
Wavelength1
- Utilizing our energy-sensitive detectors, we can measure the X-ray wavelength, eliminating the need for monochromatic X-rays. (advacam.com)
Crystalline solid1
- Powder X-ray diffraction (XRD) also obtains a diffraction pattern for the bulk material of a crystalline solid, rather than of a single crystal, which doesn't necessarily represent the overall material. (libretexts.org)
Single8
- The distinction between powder and single crystal diffraction is the degree of texturing in the sample. (wikipedia.org)
- Single Crystal, Powder Diffraction and High Pressure Crystallography. (msu.edu)
- Powder diffraction is often easier and more convenient than single crystal diffraction since it does not require individual crystals be made. (libretexts.org)
- The upgrade of the beamline was completed with the delivery of three new detectors for fast and ultrafast imaging down to the time scale of a single X-ray pulse. (esrf.fr)
- Our cameras are based on cutting-edge single X-ray photon counting sensors, and each detected photon is processed individually. (advacam.com)
- Instead of taking a single diffraction image accumulating all X-ray energies (wavelengths) into a single image as performed in the traditional XRD apparatus, we record about 150 images at once. (advacam.com)
- The basic principle of the "Energy Dispersive X-ray Diffraction" (EDXRD) in transmission geometry: The spectral sensitivity of our detectors enables us to record dozen of images during a single measurement. (advacam.com)
- Our advanced single-particle counting cameras, combined with Energy Dispersive X-ray Diffraction (EDXRD) technology, allow for rapid scanning of the entire volume of a mineral sample within milliseconds. (advacam.com)
Radiation1
- To inspect the material's volume, harder X-ray radiation is necessary. (advacam.com)
Materials1
- The SCS is organising the ICDD® Workshop on 'Materials Characterization Using Powder X-ray Diffraction' under 'Goa University Crystallography Workshop' series. (unigoa.ac.in)
Beamline1
- The beamline utilizes a pair of Silicon X-ray mirrors (length 800 mm, distance: 1000 mm) with three stripes (Chromium, Silicon and Platinum) for higher harmonic suppression. (wayforlight.eu)
Atomic1
- Because the sample itself is acting as the diffraction grating, this spacing is the [atomic spacing]. (wikipedia.org)
Optics1
- The well-established way to obtain the ultimate resolution is to use X-ray optics. (excillum.com)