A comparative study of the static and kinetic frictional resistance of titanium molybdenum alloy archwires in stainless steel brackets.
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This ex vivo study compared the static and kinetic frictional resistance of eight different archwires tested in a single, stainless steel, zero base 0.022 x 0.028 inch (0.56 x 0.711 mm) slot standard edgewise bracket. The archwires evaluated were 0.019 x 0.025 inch (0.483 x 0.636 mm) in dimension, manufactured from the following alloys: beta titanium (TMA), 'low friction' coloured beta titanium (aqua, honeydew, purple and violet), ion-implanted beta titanium, Timolium and a stainless steel control. Prior to friction testing, bracket and archwire dimensions were measured by direct digital imaging via a desktop computer linked to a binocular light microscope. Frictional force was evaluated using an Instron universal testing machine. All experiments were carried out at room temperature, with no ligation, in the dry state with 20 degrees of added torque. The results demonstrated that static and kinetic friction were statistically significant (P < 0.001) for all archwire types. Ion-implanted and standard TMA archwires were found to have no significant advantage over stainless steel. The archwire alloys may be ranked as follows: stainless steel produced the lowest frictional resistance followed by honeydew, ion-implanted TMA and Timolium, with aqua, purple and violet producing frictional resistance values as high as standard TMA. It was also found that the percentage difference between the archwire and bracket slot dimensions claimed by the manufacturers and those measured in this experiment produced tolerances ranging from +5.37 to -6.67 per cent. (+info)
Corrosion behavior of dental alloys in various types of electrolyzed water.
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The corrosion behavior of dental alloys was examined in electrolyzed strong acid water, weak acid water and neutral water using a 7-day immersion test. The precious metal alloys, gold alloy. Au-Ag-Pd alloy and silver alloy showed the greatest surface color change and dissolution of constituents in the strong acid water and the smallest in the neutral water. The release of Au from gold alloy was especially marked in the strong acid water. Co-Cr alloy showed greater corrosion and tarnish resistance in the strong acid water rather than in the weak acid water and the neutral water. X-ray microanalysis revealed that the corrosion products on the precious metal alloys were silver chloride crystals and the thin brown products on Co-Cr alloy were cobalt and chromium oxides. Ti was sound in all three types of electrolyzed water. The neutral water appeared the least corrosive to metals among the three types showing equivalent bactericidal activity. (+info)
Setting and flexural properties of metal-resin composite using Ag-Cu particles as filler and chemical accelerator.
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A metal-resin composite material was experimentally prepared by mixing a powder consisting of Ag-Cu particles and BPO with a paste consisting of UDMA-based monomer and 4-META in the absence of tertiary amine. The working time and setting time were mainly affected by the amounts of 4-META, BPO and metal particles, most of them fulfilling the requirements for working time and setting time specified in ISO 4049:2000 in the present experimental conditions. The flexural strength ranged from 49.6 MPa to 77.8 MPa, and the highest value was obtained when the 4-META concentration was high and metal particle content was low. The flexural modulus of elasticity, ranging from 6.7 GPa to 11.9 GPa, significantly increased as the 4-META concentration and metal particle content increased. Based on its mechanical properties, this metal-resin composite in which metal particles are involved in the polymerization initiation system has the potential to be used as a dental restorative material. (+info)
Effect of cement types on the tensile strength of metallic crowns submitted to thermocycling.
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The relationship between metallic cast crowns and tensile strength according to cement types submitted to thermocycling was studied. Seventy-two metallic crowns were cast with Verabond II Ni-Cr alloy and cemented in standardized preparations with 10 masculine tapering. Three types of finishing line (45-degree chamfered, 20-degree bevel shoulder and right shoulder) were made with diamond burs on bovine teeth. Twenty-four metallic crowns in each group were randomly subdivided into three subgroups of 8 samples each according to the cement used: SS White zinc phosphate cement, Vitremer resin-modified glass ionomer cement, and Rely X resin cement and were submitted to thermocycling. Retention was evaluated according to tensile load required to displace the metallic cast crowns from tooth preparations with an Instron testing machine. ANOVA and Tukey's test showed a statistically significant difference among luting materials, with greater results for Rely X resin cement (24.9 kgf) followed by SS White zinc phosphate cement (13.3 kgf) and Vitremer resin-modified glass ionomer cement (10.1 kgf). The finishing line types did not influence the tensile resistance of the crowns fixed with the three cements. Increased tensile resistance of metallic crowns fixed on bovine teeth was obtained with resin cement, independent of the finishing line types. (+info)
Evaluation of the adaptation interface of one-piece implant-supported superstructures obtained in Ni-Cr-Ti and Pd-Ag alloys.
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Several formulations of alternative alloys have been proposed for the substitution of gold-based alloys used in Dentistry. Recently, a Ni-Cr-Ti-based alloy has been introduced. The purpose of this work was to verify the marginal adaptation obtained with one-piece superstructures for implant-supported prostheses obtained in Ni-Cr-Ti alloy, compared to a semi-noble alloy Pd-Ag. Eight superstructures for each alloy were produced over 4 implants in the anterior region of the mandible. The superstructures were placed in a torquemeter and the fixation screw of implant #1 was tightened with a 20 Ncm load with the others loosened (Sheffield test). The unfitness (in mm) was measured using a three-dimensional optical measurer in each implant, in the buccal and lingual aspects. The obtained data were submitted to statistical analysis by the analysis of variance and Tukey's test at 5% level. Significant differences were found for the factors material (p< or =0.05), with Ni-Cr-Ti pieces better than Pd-Ag ones, and implants (p< or =0.01). There were no significant differences for the factor position and interactions among factors (p>0.05). Based on the analysis of the data, it is possible to conclude that the Ni-Cr-Ti alloy makes possible the obtainment of one-piece implant-supported superstructures with a smaller misfit compared to the one obtained in Pd-Ag alloy, traditionally indicated for this situation. Additional tests may verify the superiority of the Ni-Cr-Ti alloy. (+info)
Dynamic frictional behaviour of orthodontic archwires and brackets.
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The aim of this study was to evaluate the frictional behaviour of 15 different archwires and 16 different brackets using small oscillating displacements when opposed to a standard stainless steel bracket or a standard stainless steel wire. Tests were run according to a pilot study at a frequency of 1 Hz and with a reciprocating tangential displacement of 200 microm, while the wire remained centred in the bracket slot under a load of 2 N. The results indicated a significant difference between the evaluated wires and brackets. The mean coefficient of friction (COF) of the wires varied from 0.16 for Imagination NiTi tooth-coloured wire to 0.69 for the True Chrome Resilient Purple wire, while for the brackets it ranged from 0.39 for Ultratrimm to 0.72 for the Master Series. The fact that in this study, a large number of different commercially available archwires and brackets were evaluated with the same apparatus according to the same protocol, allows a direct comparison of the different archwire and bracket combinations, and can assist in the choice of the optimal bracket-wire combination with regard to friction. (+info)
Metal ion release from new and recycled stainless steel brackets.
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As orthodontic appliances can corrode with time in the oral environment, the aim of this study was to compare the release of metal ions from new and recycled brackets immersed in buffers of different pH values over a 48 week period. To simulate commercial recycling, the stainless steel brackets were divided into two groups: new and recycled. The bases of the latter were coated with adhesive and the brackets were heat treated before being immersed in the test solution for 48 weeks. The release of nickel, chromium, iron, copper, cobalt and manganese ions was analysed by atomic absorption spectrophotometry. Differences were compared using one-way analysis of variance. The results showed that recycled brackets released more ions than new brackets (P < 0.05). Brackets immersed in solutions of pH 4 released more ions than those immersed in solutions of pH 7, and the total amount of ions released increased with time over the 48 week period (P < 0.05). This study demonstrates that both new and recycled brackets will corrode in the oral environment. To avoid clinical side-effects, metal brackets should be made more resistant to corrosion, and recycled brackets should not be used. (+info)
Machinability evaluation of titanium alloys.
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In the present study, the machinability of titanium, Ti-6Al-4V, Ti-6A1-7Nb, and free-cutting brass was evaluated using a milling machine. The metals were slotted with square end mills under four cutting conditions. The cutting force and the rotational speed of the spindle were measured. The cutting forces for Ti-6Al-4V and Ti-6Al-7Nb were higher and that for brass was lower than that for titanium. The rotational speed of the spindle was barely affected by cutting. The cross sections of the Ti-6Al-4V and Ti-6Al-7Nb chips were more clearly serrated than those of titanium, which is an indication of difficult-to-cut metals. There was no marked difference in the surface roughness of the cut surfaces among the metals. Cutting force and the appearance of the metal chips were found to be useful as indices of machinability and will aid in the development of new alloys for dental CAD/CAM and the selection of suitable machining conditions. (+info)